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No, mothballs do not keep bats away. Not only are mothballs completely ineffective when repelling or removing bats, but using them could be illegal, depending on where you live. Remember, bats are federally protected, and it's illegal to use chemicals during the removal process, and mothballs tend to fall into this category.

Trees that provide a habitat to bats and an abundance of bugs—their main food source—will attract bats to your yard. Because the North American landscape has changed so much in recent years, bats have a harder time finding trees with cavities to shelter in. If your yard has a dead or dying tree with a lot of sun exposure, bats will likely be drawn to it because trees with those features are less common.

Once the animals and their young are out of the house, remove the nest and locate any entry points. Some may be difficult to find because some animals can fit through very small holes. Once you’ve located as many entry points as possible, use materials such as metal or masonry to block off the entry. Ideally, you should choose materials that most animals cannot chew through. Create a one-way door or flap to allow animals to leave but not return. Additional methods include using repellants designed to make an area unappealing to the types of animals that find your home so inviting. 

You can find a variety of humane bird repellent sprays online and at home improvement stores. However, if you want to try a DIY method that will keep birds away without harming them, mix some water, dish soap, and a few drops of peppermint oil and spray the area you want bird-free. Peppermint oil is a notoriously lovely smell for humans, but birds tend to avoid it.